NDLI: Microwave-Promoted Solid-Acid-Catalyzed One-Pot Synthesis of Phthalazinones

Content Provider	Scilit
Author	Török, Béla Outerbridge, Verona Landge, Shainaz Tamaki, Hiroko
Copyright Year	2009
Description	A one-pot, solid-acid-catalyzed, microwave-assisted synthesis of phthalazinones is described. The commercially available montmorillonite K-10 effectively catalyzed the condensation and substitution reactions. The approach was based on the direct cyclization of phthalaldehydic acid and opianic acid with substituted hydrazines. The reactions provided excellent yields and high selectivities in very short time (5-35 minutes).
Related Links	http://www.thieme-connect.de/products/ejournals/pdf/10.1055/s-0028-1088074.pdf
Ending Page	1806
Page Count	6
Starting Page	1801
ISSN	00397881
e-ISSN	1437210X
DOI	10.1055/s-0028-1088074
Journal	Synthesis
Issue Number	11
Volume Number	2009
Language	English
Publisher	Georg Thieme Verlag KG
Publisher Date	2009-04-27
Access Restriction	Open
Subject Keyword	Journal: Synthesis Organic Chemistry Phthalaldehydic Acid Montmorillonite K-10 Microwave Heating
Content Type	Text
Resource Type	Article
Subject	Organic Chemistry Catalysis

Central Library (ISO-9001:2015 Certified)
Indian Institute of Technology Kharagpur
Kharagpur, West Bengal, India | PIN - 721302

See location in the Map
03222 282435
Mail: support@ndl.gov.in

Sl.	Authority	Responsibilities	Communication Details
1	Ministry of Education (GoI), Department of Higher Education	Sanctioning Authority	https://www.education.gov.in/ict-initiatives
2	Indian Institute of Technology Kharagpur	Host Institute of the Project: The host institute of the project is responsible for providing infrastructure support and hosting the project	https://www.iitkgp.ac.in
3	National Digital Library of India Office, Indian Institute of Technology Kharagpur	The administrative and infrastructural headquarters of the project	Dr. B. Sutradhar bsutra@ndl.gov.in
4	Project PI / Joint PI	Principal Investigator and Joint Principal Investigators of the project	Dr. B. Sutradhar bsutra@ndl.gov.in Prof. Saswat Chakrabarti will be added soon
5	Website/Portal (Helpdesk)	Queries regarding NDLI and its services	support@ndl.gov.in
6	Contents and Copyright Issues	Queries related to content curation and copyright issues	content@ndl.gov.in
7	National Digital Library of India Club (NDLI Club)	Queries related to NDLI Club formation, support, user awareness program, seminar/symposium, collaboration, social media, promotion, and outreach	clubsupport@ndl.gov.in
8	Digital Preservation Centre (DPC)	Assistance with digitizing and archiving copyright-free printed books	dpc@ndl.gov.in
9	IDR Setup or Support	Queries related to establishment and support of Institutional Digital Repository (IDR) and IDR workshops	idr@ndl.gov.in

Microwave-Promoted Solid-Acid-Catalyzed One-Pot Synthesis of Phthalazinones