NDLI: Total Synthesis of (±)-Cephalosol via Silyl Enol Ether Acylation

Content Provider	Scilit
Author	Koert, Ulrich Arlt, Alexander
Copyright Year	2010
Description	An efficient total synthesis of (±)-cephalosol is reported. Key steps are the acylation of a silyl enol ether with monomethyl oxalyl chloride and the subsequent acid-mediated ring closure to the isocoumarin structure. A chemoselective allylation and the conversion of the olefin into a methyl acetate were applied to install the γ-lactone moiety.
Related Links	http://www.thieme-connect.de/products/ejournals/pdf/10.1055/s-0029-1218647.pdf
Ending Page	922
Page Count	6
Starting Page	917
ISSN	00397881
e-ISSN	1437210X
DOI	10.1055/s-0029-1218647
Journal	Synthesis
Issue Number	06
Volume Number	2010
Language	English
Publisher	Georg Thieme Verlag KG
Publisher Date	2010-01-12
Access Restriction	Open
Subject Keyword	Journal: Synthesis Organic Chemistry
Content Type	Text
Resource Type	Article
Subject	Organic Chemistry Catalysis

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