NDLI: A Simple Practical Method for the Synthesis of 4,6-Dimethoxy-1,3,5-triazin-2(1H)-one Using Dimethylamine-Functionalized Solid-Phase Reagents

Content Provider	Scilit
Author	Kunishima, Munetaka Hioki, Kazuhito Ohshima, Keiichi Sota, Yuko Tanaka, Miki
Copyright Year	2009
Description	A simple practical method for the synthesis of 4,6-dimethoxy-1,3,5-triazin-2(1H)-one was developed. The desired product was easily obtained from 2-chloro-4,6-dimethoxy-1,3,5-triazine and acetic acid by shaking with dimethylamine-functionalized silica gel in ethanol. It was also demonstrated that the silica gel could be recycled by washing it with diluted aqueous ammonia solution.
Related Links	http://www.thieme-connect.de/products/ejournals/pdf/10.1055/s-0028-1083330.pdf
Ending Page	544
Page Count	3
Starting Page	542
ISSN	00397881
e-ISSN	1437210X
DOI	10.1055/s-0028-1083330
Journal	Synthesis
Issue Number	04
Volume Number	2009
Language	English
Publisher	Georg Thieme Verlag KG
Publisher Date	2009-01-27
Access Restriction	Open
Subject Keyword	Journal: Synthesis Organic Chemistry Supported Reagents Nucleophilic Aromatic Substitutions
Content Type	Text
Resource Type	Article
Subject	Organic Chemistry Catalysis

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A Simple Practical Method for the Synthesis of 4,6-Dimethoxy-1,3,5-triazin-2(1H)-one Using Dimethylamine-Functionalized Solid-Phase Reagents