NDLI: Room-temperature synthesis of Prussian blue analogue Co3[Co(CN)6]2 porous nanostructures and their CO2 storage properties

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Room-temperature synthesis of Prussian blue analogue Co₃[Co(CN)₆]₂ porous nanostructures and their CO₂ storage properties

Content Provider	Royal Society of Chemistry (RSC)
Author	Hu, Lin Yan, Nan Chen, Qian-wang Mei, Ji-yang Zhang, Ping
Copyright Year	2011
Abstract	A nanosized Prussian blue analogue Co3[Co(CN)6]2 (PBA) with novel morphology was achieved at room temperature by simple mixing K3[Co(CN)6]2 and Co(CH3COO)2·4H2O in the presence of sodium dodecylbenzenesulfonate (SDBS). The as-prepared product was characterized by X-ray powder diffraction (XRD), field emission scanning electron microscopy (FE-SEM), and transmission electron microscopy (TEM). The effects of synthetic parameters such as different surfactants on the morphology and size of the particles were investigated. The experimental results showed that the amount of SDBS employed in the reaction system played an important role in determining the size and shape of the products. More interestingly, the as-prepared product showed high CO2 adsorption at room temperature and 1 bar of pressure, which is higher than that of the bulk materials. These results prove that the gas adsorption properties of Co3[Co(CN)6]2 are highly dependent on not only its surface area but also its morphology, and the materials at the nanoscale are more favorable to adsorption applications.
Starting Page	1574
Ending Page	1578
Page Count	5
File Format	HTM / HTML PDF
ISSN	20462069
Volume Number	1
Issue Number	8
Journal	RSC Advances
DOI	10.1039/c1ra00624j
Language	English
Publisher	Royal Society of Chemistry
Access Restriction	Open
Subject Keyword	Philippine Basketball Association Transmission electron microscopy Adsorption X-ray scattering techniques Prussian blue Powder diffraction Scanning electron microscope PBA Sodium dodecylbenzenesulfonate
Content Type	Text
Resource Type	Article
Subject	Chemistry Chemical Engineering

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