NDLI: Hydroxyl telechelic building blocks from fatty acid methyl esters for the synthesis of poly(ester/amide urethane)s with versatile properties

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Hydroxyl telechelic building blocks from fatty acid methyl esters for the synthesis of poly(ester/amide urethane)s with versatile properties

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Back cover

Polymer Chemistry Vol - 3 Issue - 8

Polymer Chemistry Vol - 3 Issue - 7

Polymer Chemistry Vol - 3 Issue - 6

Polymer Chemistry Vol - 3 Issue - 5

Polymer Chemistry Vol - 3 Issue - 4

Polymer Chemistry Vol - 3 Issue - 3

Polymer Chemistry Vol - 3 Issue - 2

Polymer Chemistry Vol -2

Polymer Chemistry Vol -1

Hydroxyl telechelic building blocks from fatty acid methyl esters for the synthesis of poly(ester/amide urethane)s with versatile properties

Content Provider	Royal Society of Chemistry (RSC)
Author	Maisonneuve, Lise Lebarbé, Thomas Cloutet, Eric Gadenne, Benoit Nguyen, Thi Hang Nga Cramail, Henri Alfos, Carine
Copyright Year	2012
Abstract	A series of bio-based diols containing ester, ester–amide and amide linkages were synthesized from methyl undecenoate (derived from ricin oil) and methyl oleate (derived from sunflower oil). These polymerization grade monomers were thoroughly characterized by FTIR-ATR, NMR spectroscopy and GC. A plethora of thermoplastic polyurethanes (TPUs) with tuned thermo-mechanical properties were prepared by combining the various diols and the diisocyanates, IPDI and MDI. The structural and thermo-mechanical characterizations of PUs were performed by means of FTIR-ATR, SEC, DSC, TGA, DMA, WAXS and tensile-test experiments. As expected, the PUs displayed amorphous to semi-crystalline features with respect to the nature of the diols and diisocyanates. Modulated DSC revealed glass transition temperatures in the range of −27 °C to 63 °C as well as melt crystallization of metastable phases upon heating. The incorporation of amide functions into the PUs enhanced the Young's modulus from 287 MPa to 775 MPa, while the elongation at break decreased from 269% to 41%. A complex degradation behavior of these PUs was observed by TGA above 280 °C.
Starting Page	2583
Ending Page	2595
Page Count	13
File Format	HTM / HTML PDF
ISSN	17599954
Volume Number	3
Issue Number	9
Journal	Polymer Chemistry
DOI	10.1039/c2py20348k
Language	English
Publisher	Royal Society of Chemistry
Access Restriction	Open
Subject Keyword	Ricin Polymerization WAXS Metastability SEC Glass transition Ester Thermoplastic polyurethane MDI Sunflower oil DSC DMA Amide Nuclear magnetic resonance Dimethylacetamide U.S. Securities and Exchange Commission
Content Type	Text
Resource Type	Article
Subject	Organic Chemistry Biochemistry Bioengineering Biomedical Engineering Polymers and Plastics

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Hydroxyl telechelic building blocks from fatty acid methyl esters for the synthesis of poly(ester/amide urethane)s with versatile properties

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Hydroxyl telechelic building blocks from fatty acid methyl esters for the synthesis of poly(ester/amide urethane)s with versatile properties