NDLI: Lamellar polymer–Li<sub>x</sub>MoO<sub>3</sub> nanocomposites via encapsulative precipitation

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Lamellar polymer–Li_xMoO₃ nanocomposites via encapsulative precipitation

Content Provider	Royal Society of Chemistry (RSC)
Author	Kannewurf, Carl R. Kanatzidis, Mercouri G. Wang, Lei Schindler, Jon
Copyright Year	1997
Abstract	With Li x MoO 3 (x=0.31–0.40) as a host material, a new family of polymer–molybdenum bronze nanocomposites has been synthesized using an exfoliation/encapsulation methodology. Nanocomposites with poly(ethylene oxide), poly(ethylene glycol), poly(propylene glycol), poly(vinylpyrrolidinone), methyl cellulose, polyacrylamide, and nylon-6 were prepared and characterized by thermal gravimetric analysis (TGA), differential scanning calorimetry (DSC), powder X-ray diffraction, FTIR spectroscopy, UV–VIS spectroscopy, variable-temperature 7 Li and 13 C solid-state NMR spectroscopy and magnetic susceptibility measurements. The electrical conductivity of these materials lies in the range from 10 -2 to 10 -7 S cm -1 , and decreases as the interlayer separation increases. The intercalated polymer imparts both mechanical strength and ease of processing to these materials. The water-soluble polymer–Li x MoO 3 nanocomposites can be cast into films and other shapes, which may provide opportunities for applications. Factors affecting the intercalation reaction and the structure of nanocomposites, such as variations in the preparation procedure, the polymer molecular mass and the annealing behaviour of the products are discussed.
Starting Page	1277
Ending Page	1283
Page Count	7
File Format	PDF
ISSN	09599428
Volume Number	7
Issue Number	7
Journal	Journal of Materials Chemistry
DOI	10.1039/a700202e
Language	English
Publisher	Royal Society of Chemistry
Access Restriction	Open
Subject Keyword	DSC Li Ethylene oxide Ethylene glycol Propylene glycol Methyl cellulose Polyacrylamide gel electrophoresis Nylon Gravimetric analysis Differential scanning calorimetry X-ray crystallography Spectroscopy Solid-state nuclear magnetic resonance Nuclear magnetic resonance Magnetic susceptibility Electrical resistivity and conductivity Polymer Molecular mass Nucleic acid thermodynamics
Content Type	Text
Resource Type	Article
Subject	Chemistry Materials Chemistry

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