NDLI: Towards the use of ICP-OES for the elemental analysis of organic compounds such as glucosamine

Please wait, while we are loading the content...

A novel strategy for sequential analysis of gold nanoparticles and gold ions in water samples by combining magnetic solid phase extraction with inductively coupled plasma mass spectrometry

Towards the use of ICP-OES for the elemental analysis of organic compounds such as glucosamine

Accurate determination of small spot X-ray tube spectra by means of direct measurement in a calibrated instrumental setup

Fundamental properties of a non-destructive atmospheric-pressure plasma jet in argon or helium and its first application as an ambient desorption/ionization source for high-resolution mass spectrometry

An inter-laboratory comparison of high precision stable isotope ratio measurements for nanoparticle tracing in biological samples

The influence of menstrual blood loss and age on the isotopic composition of Cu, Fe and Zn in human whole blood

Analysis of stable isotope ratios of Ba by double-spike standard-sample bracketing using multiple-collector inductively coupled plasma mass spectrometry

The coordination core of Ag(i) N-heterocyclic carbene (NHC) complexes with anticancer properties as revealed by synchrotron radiation X-ray absorption spectroscopy

Atmospheric helium capillary dielectric barrier discharge for soft ionization: broadening of spectral lines, gas temperature and electron number density

High-efficiency photooxidation vapor generation of osmium for determination by inductively coupled plasma-optical emission spectrometry

Determination of the nitrogen abundance in organic materials by NanoSIMS quantitative imaging

Precise tellurium isotope analysis by negative thermal ionization mass spectrometry (N-TIMS)

A simplified protocol for measurement of Ca isotopes in biological samples

Signal enhancement in laser ablation inductively coupled plasma-mass spectrometry using water and/or ethanol vapor in combination with a shielded torch

Rapid identification of phosphorus containing proteins in electrophoresis gel spots by Laser-Induced Breakdown Spectroscopy, LIBS

Accurate analysis of indium–zinc oxide thin films via laser-induced breakdown spectroscopy based on plasma modeling

The effect of paraformaldehyde fixation and sucrose cryoprotection on metal concentration in murine neurological tissue

Optimizing gated detection in high-jitter kilohertz powerchip laser-induced breakdown spectroscopy

First experimental proof of asymmetric charge transfer in ICP-MS/MS (ICP-QQQ-MS) through isotopically enriched oxygen as cell gas

Back cover

Journal of Analytical Atomic Spectrometry Vol - 29 Issue - 2

Journal of Analytical Atomic Spectrometry Vol -19

Journal of Analytical Atomic Spectrometry Vol -11

Journal of Analytical Atomic Spectrometry Vol -9

Journal of Analytical Atomic Spectrometry Vol -8

Journal of Analytical Atomic Spectrometry Vol -7

Journal of Analytical Atomic Spectrometry Vol -6

Journal of Analytical Atomic Spectrometry Vol -5

Journal of Analytical Atomic Spectrometry Vol -4

Journal of Analytical Atomic Spectrometry Vol -2

Towards the use of ICP-OES for the elemental analysis of organic compounds such as glucosamine

Content Provider	Royal Society of Chemistry (RSC)
Author	Anastassiades, Tassos Makonnen, Yoseif Beauchemin, Diane Odenigbo, Chukwudum Asfaw, Alemayehu
Copyright Year	2014
Abstract	Inductively coupled plasma optical emission spectrometry with a long demountable torch (whose outer tube is 2.5 cm longer than a standard torch) and a conventional pneumatic nebulisation system was applied to the determination of C, H and O concentrations from an organic compound dissolved in water. The sample solution was simply aspirated directly into the plasma without any sample pre-treatment (such as desolvation or degassing). The long torch was required to significantly decrease the background arising from entrained air. Good linearity was obtained for C, N, H and O upon calibration with standard solutions prepared from ultrapure tris(hydroxymethyl)aminomethane. A weighed blank correction was applied to compensate for the contribution from water, especially in the cases of H and O. Under these conditions, the detection limits for C, N, H and O were, respectively, 0.2, 50, 1000 and 2000 μmol of analyte per g of solution. Accurate concentrations, according to a Student's t test at the 95% confidence level, were measured for C, H and O in a solution of D-glucosamine hydrochloride. No internal standardisation was necessary. However, the N concentration was biased high, irrespectively of the N emission line used (from 149.262 to 593.178 nm), which rules out spectroscopic interference and will be further investigated. Nonetheless, the possibility of accurately determining C, H and O simultaneously with trace elements makes the approach quite promising. It is much simpler than alternate methods that require derivatisation of the compound prior to detection.
Starting Page	454
Ending Page	457
Page Count	4
File Format	HTM / HTML PDF
ISSN	02679477
Volume Number	29
Issue Number	3
Journal	Journal of Analytical Atomic Spectrometry
DOI	10.1039/c3ja50246e
Language	English
Publisher	Royal Society of Chemistry
Access Restriction	Open
Subject Keyword	Inductively coupled plasma Organic compound Pulmonary aspiration Blood plasma Analyte Glucosamine
Content Type	Text
Resource Type	Article
Subject	Spectroscopy Analytical Chemistry

Sl.	Authority	Responsibilities	Communication Details
1	Ministry of Education (GoI), Department of Higher Education	Sanctioning Authority	https://www.education.gov.in/ict-initiatives
2	Indian Institute of Technology Kharagpur	Host Institute of the Project: The host institute of the project is responsible for providing infrastructure support and hosting the project	https://www.iitkgp.ac.in
3	National Digital Library of India Office, Indian Institute of Technology Kharagpur	The administrative and infrastructural headquarters of the project	Dr. B. Sutradhar bsutra@ndl.gov.in
4	Project PI / Joint PI	Principal Investigator and Joint Principal Investigators of the project	Dr. B. Sutradhar bsutra@ndl.gov.in Prof. Saswat Chakrabarti will be added soon
5	Website/Portal (Helpdesk)	Queries regarding NDLI and its services	support@ndl.gov.in
6	Contents and Copyright Issues	Queries related to content curation and copyright issues	content@ndl.gov.in
7	National Digital Library of India Club (NDLI Club)	Queries related to NDLI Club formation, support, user awareness program, seminar/symposium, collaboration, social media, promotion, and outreach	clubsupport@ndl.gov.in
8	Digital Preservation Centre (DPC)	Assistance with digitizing and archiving copyright-free printed books	dpc@ndl.gov.in
9	IDR Setup or Support	Queries related to establishment and support of Institutional Digital Repository (IDR) and IDR workshops	idr@ndl.gov.in

Towards the Use of Inductively Coupled Plasma Optical Emission Spectrometry for the Elemental Analysis of Organic Compounds such as Glucosamine

Improvement of the capabilities of solid sampling ETV-ICP-OES by coupling ETV to a nebulisation/pre-evaporation system

Inductively coupled plasma–microwave induced plasma tandem source for atomic emission spectrometry

High pressure asher (HPA-S) decomposition of biodiesel samples for elemental analysis by inductively coupled plasma optical emission spectrometry (ICP OES)

A novel approach to understanding the effect of matrix composition on analyte emission in an inductively coupled plasma

Use of the Hildebrand grid nebuliser for analysis of high matrix solutions containing easily ionisable elements with inductively coupled plasma mass spectrometry

Design considerations for a pressure-differential tandem source for use in atomic spectrometry

Multi-element analysis of Macedonian wines by inductively coupled plasma–mass spectrometry (ICP–MS) and inductively coupled plasma–optical emission spectrometry (IP–OES) for regional classification

Elemental and isotopic analysis of americium in non-separated spent fuels using high resolution ICP-OES and sector field ICP-MS

Towards the use of ICP-OES for the elemental analysis of organic compounds such as glucosamine

Similar Documents

Towards the Use of Inductively Coupled Plasma Optical Emission Spectrometry for the Elemental Analysis of Organic Compounds such as Glucosamine

Improvement of the capabilities of solid sampling ETV-ICP-OES by coupling ETV to a nebulisation/pre-evaporation system

Inductively coupled plasma–microwave induced plasma tandem source for atomic emission spectrometry

High pressure asher (HPA-S) decomposition of biodiesel samples for elemental analysis by inductively coupled plasma optical emission spectrometry (ICP OES)

A novel approach to understanding the effect of matrix composition on analyte emission in an inductively coupled plasma

Use of the Hildebrand grid nebuliser for analysis of high matrix solutions containing easily ionisable elements with inductively coupled plasma mass spectrometry

Design considerations for a pressure-differential tandem source for use in atomic spectrometry

Multi-element analysis of Macedonian wines by inductively coupled plasma–mass spectrometry (ICP–MS) and inductively coupled plasma–optical emission spectrometry (IP–OES) for regional classification

Elemental and isotopic analysis of americium in non-separated spent fuels using high resolution ICP-OES and sector field ICP-MS

Towards the use of ICP-OES for the elemental analysis of organic compounds such as glucosamine