NDLI: Determination of trace elements in solid plastic materials by laser ablation–inductively coupled plasma mass spectrometry

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Letters ( Journal of Analytical Atomic Spectrometry Vol - 6 Issue - 2 )

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Journal of Analytical Atomic Spectrometry Vol - 6 Issue - 1

Journal of Analytical Atomic Spectrometry Vol -5

Journal of Analytical Atomic Spectrometry Vol -4

Journal of Analytical Atomic Spectrometry Vol -2

Determination of trace elements in solid plastic materials by laser ablation–inductively coupled plasma mass spectrometry

Content Provider	Royal Society of Chemistry (RSC)
Author	Tye, Chris Abell, Ian Franks, Jeff Marshall, John
Copyright Year	1991
Abstract	The application of laser ablation inductively coupled plasma mass spectrometry (ICP-MS) to the direct determination of trace elements in solid plastic materials has been studied. A neodymium:yttrium aluminium garnet (Nd:YAG) laser was used to ablate the samples and the particulate matter thus produced was transported to the plasma torch of the ICP-MS system for measurement. The system was applied to the examination of polypropylene, polyester, poly(vinyl chloride), nylon and polyethylene, containing a variety of fillers and other additives. It was found that by using carbon-13 as an internal standard, in order to adjust for variations in ablation and transport of the different sample types, semi-quantitative analysis could be achieved with an accuracy that was within a factor of 2 of the known value for most of the elements investigated. Quantitative measurements made using laser ablation–ICP-MS, and with calibration standards of matrix composition similar to that of the materials being analysed, showed good agreement with known values. The application of the technique to the investigation of the spatial distribution of elements is briefly explored.
Starting Page	145
Ending Page	150
Page Count	6
File Format	PDF
ISSN	02679477
Volume Number	6
Issue Number	2
Journal	Journal of Analytical Atomic Spectrometry
DOI	10.1039/JA9910600145
Language	English
Publisher	Royal Society of Chemistry
Access Restriction	Open
Subject Keyword	Laser ablation Inductively coupled plasma mass spectrometry Neodymium Yttrium aluminium garnet Laser Thermal spraying Polypropylene Polyester Vinyl chloride Nylon Polyethylene Carbon-13 Ablation Composite material
Content Type	Text
Resource Type	Article
Subject	Spectroscopy Analytical Chemistry

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