NDLI: Acquisition of fast transient signals in ICP-MS with enhanced time resolution

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Acquisition of fast transient signals in ICP-MS with enhanced time resolution

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Journal of Analytical Atomic Spectrometry Vol - 31 Issue - 7

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Acquisition of fast transient signals in ICP-MS with enhanced time resolution

Content Provider	Royal Society of Chemistry (RSC)
Author	Cowen, K. Makella Managh, Amy J. Sharp, Barry L. Reid, Helen J. Douglas, David N.
Copyright Year	2016
Abstract	In recent years, the field of ICP-MS has seen an increasing trend towards sampling systems and methods that produce short transient signals, rather than a continuous signal response. Fast data acquisition, readout and storage are crucial to take advantage of the wealth of information available from these approaches. However, many of the current generation mass spectrometers, in particular sector-field instruments, were not designed to cope with such short duration signals. This article reports the use of a commercially available multi-channel scaler board, which facilitates capture of TTL pulses from an ICP-MS detector at a user defined time resolution down to 100 ns. The board was used to profile 400–600 μs wide signals with 10 μs resolution, derived from the nebulisation of a 50 nm gold nanoparticle suspension. Furthermore, the benefit of a 100% duty cycle was demonstrated for ∼10 ms wide signals, following ablation of individual macrophage cells with a fast response LA-ICP-MS interface.
Starting Page	1688
Ending Page	1692
Page Count	5
File Format	HTM / HTML PDF
ISSN	02679477
Volume Number	31
Issue Number	8
Journal	Journal of Analytical Atomic Spectrometry
DOI	10.1039/c6ja00140h
Language	English
Publisher	Royal Society of Chemistry
Access Restriction	Open
Subject Keyword	Through-the-lens metering Nanoparticle Duty cycle Ablation Macrophage
Content Type	Text
Resource Type	Article
Subject	Spectroscopy Analytical Chemistry

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