NDLI: Characterization of a helium discharge for hollow anode furnace atomization non-thermal excitation spectrometry

Please wait, while we are loading the content...

Determination of lead by electrothermal vaporization microwave-induced plasma atomic emission spectrometry after flow-through electrolytic deposition in a graphite tube packed with reticulated vitreous carbon

Diagnostic investigations of aerosols with varying water content in inductively coupled plasma mass spectrometry

Determination of trace metals in concentrated brines using inductively coupled plasma mass spectrometry on-line preconcentration and matrix elimination with flow injection

Isotope ratios of calcium determined in calcium-46 enriched samples from infants by automated multiple-collector thermal ionization mass spectrometry

Evaluation of linear photodiode array detection for continuum source atomic absorption spectrometry with electrothermal atomization

In situ concentration of selenium and tellurium hydrides in a silver-coated graphite atomizer

Comparison of chemical modifiers for simultaneous determination of different selenium compounds in serum and urine by Zeeman-effect electrothermal atomic absorption spectrometry

Mineralization of biological materials prior to determination of total mercury by cold vapour atomic absorption spectrometry

Immobilized cysteine as a reagent for preconcentration of trace metals prior to determination by atomic absorption spectrometry

Determination of gold by slurry electrothermal atomic absorption spectrometry after preconcentration by Escherichia coli and Pseudomonas putida

Study of X-ray fluorescence spectrometry and spark ablation inductively coupled plasma atomic emission spectrometry for chromium determination in ferrochromium from bulk metal samples

Determination of traces of lutetium in geological samples by resonance ionization spectroscopy

Communication. Rapid sample preconcentration by aerosol deposition for the determination of trace elements by inductively coupled plasma spectrometry

Communication. Isotope ratio measurement by inductively coupled plasma multiple collector mass spectrometry incorporating a high efficiency nebulization system

Complementary radiofrequency glow discharge source for a commercial quadrupole mass spectrometer system

Cumulative author index

Erratum

Back matter

Journal of Analytical Atomic Spectrometry Vol - 8 Issue - 6

Journal of Analytical Atomic Spectrometry Vol - 8 Issue - 5

Journal of Analytical Atomic Spectrometry Vol - 8 Issue - 4

Journal of Analytical Atomic Spectrometry Vol - 8 Issue - 3

Journal of Analytical Atomic Spectrometry Vol - 8 Issue - 2

Journal of Analytical Atomic Spectrometry Vol - 8 Issue - 1

Journal of Analytical Atomic Spectrometry Vol -7

Journal of Analytical Atomic Spectrometry Vol -6

Journal of Analytical Atomic Spectrometry Vol -5

Journal of Analytical Atomic Spectrometry Vol -4

Journal of Analytical Atomic Spectrometry Vol -2

Characterization of a helium discharge for hollow anode furnace atomization non-thermal excitation spectrometry

Content Provider	Royal Society of Chemistry (RSC)
Author	Harnly, James M. Riby, Philip G.
Copyright Year	1993
Abstract	A discharge in He has been characterized for hollow anode furnace atomization non-thermal excitation spectrometry (HA-FANES). The small surface area of the cathode and high current densities make it possible to stabilize He discharges up to 1200 hPa using a d.c. power supply operating in the constant current mode. Current—voltage characteristics were determined for pressures up to 800 hPa. Characterization at higher pressures was not possible owing to limitations of the power supply. The release of thermionic electrons from the cathode surface at temperatures in excess of 1750 K caused a dramatic decrease in the discharge potential during the atomization cycle. Increased ohmic heating of the cathode with increased currents caused a time shift in the release of thermionic electrons. Excitation temperatures, obtained from Boltzmann plots of five He I lines, decreased slightly as a function of increasing pressure and increased as a function of increasing current. Dramatic decreases in the discharge potential were observed for high concentrations (250 mg ml–1) of NaCl. The potential decreases were too short-lived to permit the accurate measurement of excitation temperatures. Integrated analytical signals increased linearly with increasing pressure.
Starting Page	945
Ending Page	953
Page Count	9
File Format	PDF
ISSN	02679477
Volume Number	8
Issue Number	7
Journal	Journal of Analytical Atomic Spectrometry
DOI	10.1039/JA9930800945
Language	English
Publisher	Royal Society of Chemistry
Access Restriction	Open
Subject Keyword	Anode Cathode Pascal (unit) Thermionic emission Joule heating Spectroscopic notation
Content Type	Text
Resource Type	Article
Subject	Spectroscopy Analytical Chemistry

Sl.	Authority	Responsibilities	Communication Details
1	Ministry of Education (GoI), Department of Higher Education	Sanctioning Authority	https://www.education.gov.in/ict-initiatives
2	Indian Institute of Technology Kharagpur	Host Institute of the Project: The host institute of the project is responsible for providing infrastructure support and hosting the project	https://www.iitkgp.ac.in
3	National Digital Library of India Office, Indian Institute of Technology Kharagpur	The administrative and infrastructural headquarters of the project	Dr. B. Sutradhar bsutra@ndl.gov.in
4	Project PI / Joint PI	Principal Investigator and Joint Principal Investigators of the project	Dr. B. Sutradhar bsutra@ndl.gov.in Prof. Saswat Chakrabarti will be added soon
5	Website/Portal (Helpdesk)	Queries regarding NDLI and its services	support@ndl.gov.in
6	Contents and Copyright Issues	Queries related to content curation and copyright issues	content@ndl.gov.in
7	National Digital Library of India Club (NDLI Club)	Queries related to NDLI Club formation, support, user awareness program, seminar/symposium, collaboration, social media, promotion, and outreach	clubsupport@ndl.gov.in
8	Digital Preservation Centre (DPC)	Assistance with digitizing and archiving copyright-free printed books	dpc@ndl.gov.in
9	IDR Setup or Support	Queries related to establishment and support of Institutional Digital Repository (IDR) and IDR workshops	idr@ndl.gov.in

Furnace atomic non-thermal excitation spectrometry with the furnace as a hollow anode

Investigation of the role of hollow cathode (vaporization) temperature on the performance of particle beam/hollow cathode atomic emission spectrometry (PB-HC-AES)

Excitation Characteristics and Matrix Effect in a Helium Radiofrequency Atomization and Excitation Source for Atomic Emission Spectrometry

Local electric discharge in liquid as a source of atomization and excitation for atomic emission spectroscopy

Determination of nitrogen and oxygen and species containing nitrogen by molecular non-thermal excitation spectrometry (MONES) using microwave-induced plasma (MIP) and furnace atomization non-thermal excitation spectrometry (FANES) sources

Design and thermal analysis of the insert region heater of a lanthanum hexaboride hollow cathode

Hollow electrode plasma excitation source

Pulse optimization criteria for the microcavity hollow cathode discharge emission source

Excitation and detection of molecular species with furnace atomization plasma emission spectrometry

Characterization of a helium discharge for hollow anode furnace atomization non-thermal excitation spectrometry

Similar Documents

Furnace atomic non-thermal excitation spectrometry with the furnace as a hollow anode

Investigation of the role of hollow cathode (vaporization) temperature on the performance of particle beam/hollow cathode atomic emission spectrometry (PB-HC-AES)

Excitation Characteristics and Matrix Effect in a Helium Radiofrequency Atomization and Excitation Source for Atomic Emission Spectrometry

Local electric discharge in liquid as a source of atomization and excitation for atomic emission spectroscopy

Determination of nitrogen and oxygen and species containing nitrogen by molecular non-thermal excitation spectrometry (MONES) using microwave-induced plasma (MIP) and furnace atomization non-thermal excitation spectrometry (FANES) sources

Design and thermal analysis of the insert region heater of a lanthanum hexaboride hollow cathode

Hollow electrode plasma excitation source

Pulse optimization criteria for the microcavity hollow cathode discharge emission source

Excitation and detection of molecular species with furnace atomization plasma emission spectrometry

Characterization of a helium discharge for hollow anode furnace atomization non-thermal excitation spectrometry