NDLI: Synthesis of high surface area CuMn<sub>2</sub>O<sub>4</sub> by supercritical anti-solvent precipitation for the oxidation of CO at ambient temperature

Please wait, while we are loading the content...

Catalysis Science & Technology Vol -7

Catalysis Science & Technology Vol -6

Catalysis Science & Technology Vol -5

Catalysis Science & Technology Vol -4

Catalysis Science & Technology Vol -3

Catalysis Science & Technology Vol -2

Catalysis Science & Technology Vol -1

Catalysis Science & Technology Vol - 1 Issue - 9

Catalysis Science & Technology Vol - 1 Issue - 8

Catalysis Science & Technology Vol - 1 Issue - 7

Catalysis Science & Technology Vol - 1 Issue - 6

Catalysis Science & Technology Vol - 1 Issue - 5

Front cover

Contents list

Studying Fischer–Tropsch catalysts using transmission electron microscopy and model systems of nanoparticles on planar supports

The main catalytic challenges in GTL (gas-to-liquids) processes

Chemocatalytic conversion of cellulose: opportunities, advances and pitfalls

Organocatalytic asymmetric transfer hydrogenation of imines

A new class of heterogeneous Pd catalysts for synthetic organic chemistry

Synthesis of high surface area CuMn₂O₄ by supercritical anti-solvent precipitation for the oxidation of CO at ambient temperature

Selective oxidation of alkenes using graphite-supported gold-palladium catalysts

Correction for a possible reversible adsorption over an “inert” material

ZnO based nanowires grown by chemical vapour deposition for selective hydrogenation of acetylene alcohols

Graphene support for enhanced electrocatalytic activity of Pd for alcohol oxidation

[VO(acac)₂] hybrid catalyst: from complex immobilization onto silica nanoparticles to catalytic application in the epoxidation of geraniol

β-Molybdenum nitride: synthesis mechanism and catalytic response in the gas phase hydrogenation of p-chloronitrobenzene

Photocatalytic degradation of Rhodamine B using nanocrystalline TiO₂–zeolite surface composite catalysts: effects of photocatalytic condition on degradation efficiency

Zn(Proline)₂: a novel catalyst for the synthesis of dicoumarols

Application of fly ash supported titanium dioxide for phenol photodegradation in aqueous solution

Experimental evidence for three rate-controlling regions of the non-oxidative methane dehydroaromatization over Mo/HZSM-5 catalyst at 1073 K

Foam, fleece and honeycomb: catalytically active coatings from colloidally prepared nanoparticles

Back cover

Catalysis Science & Technology Vol - 1 Issue - 4

Catalysis Science & Technology Vol - 1 Issue - 3

Catalysis Science & Technology Vol - 1 Issue - 2

Catalysis Science & Technology Vol - 1 Issue - 1

Synthesis of high surface area CuMn₂O₄ by supercritical anti-solvent precipitation for the oxidation of CO at ambient temperature

Content Provider	Royal Society of Chemistry (RSC)
Author	Kondrat, S. A. Bartley, J. K. Dickinson, C. Crudace, M. J. Rosseinsky, M. J. Carley, A. F. Xu, Z. Tang, Z.-R. Davies, T. E. Claridge, J. B. Hutchings, G. J. Allix, M. Romani, S. Taylor, S. H.
Copyright Year	2011
Abstract	A series of high surface area nanocrystalline copper manganese oxide catalysts have been prepared by supercritical anti-solvent (SAS) precipitation using CO2 and tested for the ambient temperature oxidation of CO. The catalysts were prepared by precipitation from an ethanol/metal acetate solution and the addition of small quantities of water was found to result in a mixed acetate precursor with surface areas >200 m2 g−1, considerably higher than those prepared by conventional precipitation methods. The surface area of the final calcined mixed oxide was found to be dependent upon the initial water concentration. XRD and FT-IR analysis indicated that the addition of water promoted the formation of carbonate species in the amorphous acetate precursor, with high resolution TEM and STEM showing the material to consist of spherical agglomerations of fibrous strings of ca. 30 nm length. This is in contrast to the material prepared in the absence of water, using the same SAS methodology, which typically yields quasi-spherical particles of 100 nm size.
Starting Page	740
Ending Page	746
Page Count	7
File Format	HTM / HTML PDF
ISSN	20444753
Volume Number	1
Issue Number	5
Journal	Catalysis Science & Technology
DOI	10.1039/c1cy00064k
Language	English
Publisher	Royal Society of Chemistry
Access Restriction	Open
Subject Keyword	X-ray crystallography String theory Transmission electron microscopy SAS Ethanol Serial Attached SCSI Supercritical fluid Calcination Fourier-transform infrared spectroscopy Copper Scanning transmission electron microscopy Manganese oxide
Content Type	Text
Resource Type	Article
Subject	Catalysis

Sl.	Authority	Responsibilities	Communication Details
1	Ministry of Education (GoI), Department of Higher Education	Sanctioning Authority	https://www.education.gov.in/ict-initiatives
2	Indian Institute of Technology Kharagpur	Host Institute of the Project: The host institute of the project is responsible for providing infrastructure support and hosting the project	https://www.iitkgp.ac.in
3	National Digital Library of India Office, Indian Institute of Technology Kharagpur	The administrative and infrastructural headquarters of the project	Dr. B. Sutradhar bsutra@ndl.gov.in
4	Project PI / Joint PI	Principal Investigator and Joint Principal Investigators of the project	Dr. B. Sutradhar bsutra@ndl.gov.in Prof. Saswat Chakrabarti will be added soon
5	Website/Portal (Helpdesk)	Queries regarding NDLI and its services	support@ndl.gov.in
6	Contents and Copyright Issues	Queries related to content curation and copyright issues	content@ndl.gov.in
7	National Digital Library of India Club (NDLI Club)	Queries related to NDLI Club formation, support, user awareness program, seminar/symposium, collaboration, social media, promotion, and outreach	clubsupport@ndl.gov.in
8	Digital Preservation Centre (DPC)	Assistance with digitizing and archiving copyright-free printed books	dpc@ndl.gov.in
9	IDR Setup or Support	Queries related to establishment and support of Institutional Digital Repository (IDR) and IDR workshops	idr@ndl.gov.in

Bioethanol selective oxidation to acetaldehyde over Ag–CeO₂: role of metal–support interactions

Gold nanorods or nanoparticles deposited on layered manganese oxide: new findings

A magnetically recoverable γ-Fe₂O₃ nanocatalyst for the synthesis of 2-phenylquinazolines under solvent-free conditions

Synthesis of high surface area CuMn2O4 by supercritical anti-solvent precipitation for the oxidation of CO at ambient temperature

A sol–gel route to synthesize SiO₂/TiO₂ well-ordered nanocrystalline mesoporous photocatalysts through ionic liquid control

Homogeneous precipitation method preparation of modified red mud supported Ni mesoporous catalysts for ammonia decomposition

Summary of Comments on Serial Attached SCSI 1.1 (SAS-1.1) Standard

Magnesium oxide nanosheets as effective catalysts for the synthesis of diethyl carbonate from ethyl carbamate and ethanol

Highly sulfonated graphene and graphene oxide nanosheets as heterogeneous nanocatalysts in green synthesis of bisphenolic antioxidants under solvent free conditions

Synthesis of high surface area CuMn₂O₄ by supercritical anti-solvent precipitation for the oxidation of CO at ambient temperature

Similar Documents

Bioethanol selective oxidation to acetaldehyde over Ag–CeO2: role of metal–support interactions

Gold nanorods or nanoparticles deposited on layered manganese oxide: new findings

A magnetically recoverable γ-Fe2O3 nanocatalyst for the synthesis of 2-phenylquinazolines under solvent-free conditions

Synthesis of high surface area CuMn2O4 by supercritical anti-solvent precipitation for the oxidation of CO at ambient temperature

A sol–gel route to synthesize SiO2/TiO2 well-ordered nanocrystalline mesoporous photocatalysts through ionic liquid control

Homogeneous precipitation method preparation of modified red mud supported Ni mesoporous catalysts for ammonia decomposition

Summary of Comments on Serial Attached SCSI 1.1 (SAS-1.1) Standard

Magnesium oxide nanosheets as effective catalysts for the synthesis of diethyl carbonate from ethyl carbamate and ethanol

Highly sulfonated graphene and graphene oxide nanosheets as heterogeneous nanocatalysts in green synthesis of bisphenolic antioxidants under solvent free conditions

Synthesis of high surface area CuMn2O4 by supercritical anti-solvent precipitation for the oxidation of CO at ambient temperature

Bioethanol selective oxidation to acetaldehyde over Ag–CeO₂: role of metal–support interactions

A magnetically recoverable γ-Fe₂O₃ nanocatalyst for the synthesis of 2-phenylquinazolines under solvent-free conditions

A sol–gel route to synthesize SiO₂/TiO₂ well-ordered nanocrystalline mesoporous photocatalysts through ionic liquid control

Synthesis of high surface area CuMn₂O₄ by supercritical anti-solvent precipitation for the oxidation of CO at ambient temperature