NDLI: A versatile, solvent-free methodology for the functionalisation of carbon nanotubes

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Synthesis and antifreeze activity of fish antifreeze glycoproteins and their analogues

Photodissociation and photoelectron imaging of molecular ions: probing multisurface and multichannel dynamics

Total synthesis of all (−)-agelastatin alkaloids

Exploiting donor–acceptor interactions in aqueous dynamic combinatorial libraries: exploratory studies of simple systems

Site-specific photocatalytic splitting of methanol on TiO₂(110)

Dissecting tunicamycin biosynthesis by genome mining: cloning and heterologous expression of a minimal gene cluster

Highly enantioselective synthesis of 1,3-bis(hydroxymethyl)-2-oxindoles from unprotected oxindoles and formalin using a chiral Nd^III complex

Site-specific PEGylation of proteins by a Staudinger-phosphite reaction

A versatile, solvent-free methodology for the functionalisation of carbon nanotubes

A tangled web—interconnecting pathways to amorphadiene and the amorphene sesquiterpenes

Ambient temperature anion-dependent spin state switching observed in “mostly low spin” heteroleptic iron(ii) diimine complexes

Photoinduced N₂ loss as a route to long-lived organometallic alkane complexes: A time-resolved IR and NMR study

Frozen-solution magnetisation dynamics of hexanuclear oxime-based Mn^III Single-Molecule Magnets

Unified synthesis of enantiopure β²h, β³h and β^2,3-amino acids

X-ray snapshots for metalloporphyrin axial ligation

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A versatile, solvent-free methodology for the functionalisation of carbon nanotubes

Content Provider	Royal Society of Chemistry (RSC)
Author	Shaffer, Milo S. P. Menner, Angelika Menzel, Robert Tran, Michael Q. Bismarck, Alexander Kay, Christopher W. M.
Copyright Year	2010
Abstract	High temperature activation of carbon nanotubes (CNTs) provides a new and highly versatile functionalisation strategy. The reaction allows the attachment of a wide variety of functional species onto the nanotube surface at grafting ratios between 1–8 wt%, whilst maintaining the intrinsic properties of the untreated materials. The underlying, radical-based, reaction mechanism has been established by quenching experiments and EPR studies. The distribution of the functionalised sites has been investigated at the microscopic scale using tagging reactions. The grafted products have been characterized by electron microscopy, thermal analysis (TGA), Raman spectroscopy, and inverse gas chromatography (IGC). The change in the CNT surface properties after grafting has been quantified in terms of dispersive and specific surface energies, and altered dispersibilities in a broad range of solvents. It is possible to carry out the reaction using gas phase reagents, providing a clean, efficient, and scalable methodology, relevant to a diverse range of applications.
Starting Page	603
Ending Page	608
Page Count	6
File Format	HTM / HTML PDF
ISSN	20416520
Volume Number	1
Issue Number	5
Journal	Chemical Science
DOI	10.1039/c0sc00287a
Language	English
Publisher	Royal Society of Chemistry
Access Restriction	Open
Subject Keyword	Carbon nanotube Transmission electron microscopy IGC EPR CNT Reaction mechanism Inverse gas chromatography Raman Thermal analysis Raman spectroscopy Grafting
Content Type	Text
Resource Type	Article
Subject	Chemistry

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A versatile, solvent-free methodology for the functionalisation of carbon nanotubes

Solvent-free microwave-assisted Bingel reaction in carbon nanohorns

Oxidation, defunctionalization and catalyst life cycle of carbon nanotubes: a Raman spectroscopy view

Single- and multi-walled carbon nanotubes covalently linked to perylenebisimides: synthesis, characterization and photophysical properties

Direct grafting of carbon nanotubes with ethylenediamine

Electron microscopy, transmission electron microscopy, thermo gravimetric analysis and raman spectroscopy.

Synthesis of covalently attached hexadecaanilines on carbon nanotubes: toward electronic nanocarbon preparation

Metal nanoparticles reveal the organization of single-walled carbon nanotubes in bundles

Anchored palladium nanoparticles onto single walled carbon nanotubes: Efficient recyclable catalyst for N-containing heterocycles

A versatile, solvent-free methodology for the functionalisation of carbon nanotubes

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