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Crystallization process development of metal–organic frameworks by linking secondary building units, lattice nucleation and luminescence: insight into reproducibility

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CrystEngComm Vol - 19 Issue - 2

Crystallization process development of metal–organic frameworks by linking secondary building units, lattice nucleation and luminescence: insight into reproducibility

Content Provider	Royal Society of Chemistry (RSC)
Author	Chang, Yun Hsuan Lee, Hung Lin Lee, Tu
Copyright Year	2017
Abstract	The interdependence of crystallinity, secondary building unit (SBU) formation, linker vacancy, crystal habit, photoluminescence, and surface area for UiO-66 and In-MIL-68, respectively, produced by different processing modes has been fully investigated and linked together to comprehend the relationships among SBU synthesis pathways, structures, and functional properties. The solid-state properties of UiO-66 were found to be process-sensitive, but those of In-MIL-68 except for crystal habits were mode independent, most likely due to the versatile Zr6(μ3-O)4(μ3-OH)4(CO2)12 SBU formation steps with more competing events for UiO-66 and the relatively straightforward {In(μ-O2CR)2(μ-OH)}∞ chain SBU formation steps for In-MIL-68. The reproducibility of the desired properties of metal–organic frameworks (MOFs) relies on the crystallization process designed for specific SBU formation and nucleation trajectory.
Starting Page	426
Ending Page	441
Page Count	16
File Format	HTM / HTML PDF
ISSN	14668033
Volume Number	19
Issue Number	3
Journal	CrystEngComm
DOI	10.1039/c6ce02246d
Language	English
Publisher	Royal Society of Chemistry
Access Restriction	Open
Subject Keyword	Processing mode Nucleation SBU Photoluminescence Crystal habit
Content Type	Text
Resource Type	Article
Subject	Chemistry Condensed Matter Physics Materials Science

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