NDLI: Simultaneous determination of seven acrylates in food contact paper products by GC/MS and modified QuEChERS

Please wait, while we are loading the content...

Sensitive analysis of phthalate esters in plastic bottled water via on-line capillary solid-phase microextraction liquid chromatography electrospray ionization-ion trap mass spectrometry

Identification of sulphur in nail polish by pattern recognition methods combined with portable energy dispersive X-ray fluorescence spectral data

A practical method for the simultaneous quantitative determination of twelve anthraquinone derivatives in rhubarb by a single-marker based on ultra-performance liquid chromatography and chemometric analysis

Deciphering the quenching mechanism of 2D MnO₂ nanosheets towards Au nanocluster fluorescence to design effective glutathione biosensors

Effect of sodium dodecyl sulphate and Brij-35 on the analysis of sulphonamides in physiological samples using direct injection and acetonitrile gradients

Simultaneous determination of seven acrylates in food contact paper products by GC/MS and modified QuEChERS

Calix[4]arene crown ether as an oriented linker for highly sensitive detection of zinc ions using a peptide probe

Modification of a disposable pencil graphite electrode with multiwalled carbon nanotubes: application to electrochemical determination of diclofenac sodium in some pharmaceutical and biological samples

Multiwalled carbon nanotubes–poly(vinyl alcohol) composite cryogel used in microcolumn liquid chromatography to separate various herbicides

Fast clean-up and selective enrichment of florfenicol in milk by restricted access media molecularly imprinted magnetic microspheres based on surface-initiated photoiniferter-mediated polymerization

Back cover

Analytical Methods Vol - 8 Issue - 9

Analytical Methods Vol - 8 Issue - 8

Analytical Methods Vol - 8 Issue - 7

Analytical Methods Vol - 8 Issue - 6

Analytical Methods Vol - 8 Issue - 5

Analytical Methods Vol -7

Analytical Methods Vol -6

Analytical Methods Vol -5

Analytical Methods Vol -4

Analytical Methods Vol -3

Analytical Methods Vol -2

Analytical Methods Vol -1

Simultaneous determination of seven acrylates in food contact paper products by GC/MS and modified QuEChERS

Content Provider	Royal Society of Chemistry (RSC)
Author	Huang, Jinfeng Xun, Zhiqing Guo, Xindong Li, Xiu-Ying Lin, Senyu He, Shuang Xian, Yanping
Copyright Year	2016
Abstract	By utilizing gas chromatography tandem mass spectrometry (GC/MS) and QuEChERS purification technology, a new method was developed for the detection of seven acrylate compounds (methyl methacrylate, butyl acrylate, sec-butyl acrylate, 2-ethylhexyl acrylate, glycidyl methacrylate, n-octyl acrylate, and N-octyl methacrylate) in food contact paper products. Hexane was used as the extraction solvent and carbon nanotubes were used as adsorbents during the QuEChERS purification. The acrylates were separated by an ultra-inert column (DB-5MS UI) and detected in the electron ionization mode of MS with selected ions monitoring (SIM). Under the optimal conditions, the calibration curves for the seven analytes were linear in the range of 5.0–1000 μg L−1 with the correlation coefficients higher than 0.9984. The quantitation limits of the method (S/N = 10) of these acrylates were in the range of 50.0–100.0 μg kg−1. The mean recoveries for paper products at three spiked concentration levels of 50.0–1000 μg kg−1 were in the range of 82.1–106.5%, and the relative standard deviations (RSDs, n = 6) ranged from 1.5% to 5.6%. This method is accurate, simple and rapid, and could be applied to the detection of acrylates in food contact paper products.
Starting Page	3953
Ending Page	3958
Page Count	6
File Format	HTM / HTML PDF
ISSN	17599660
Volume Number	8
Issue Number	19
Journal	Analytical Methods
DOI	10.1039/c6ay00613b
Language	English
Publisher	Royal Society of Chemistry
Access Restriction	Open
Subject Keyword	Carbon nanotube Gas chromatography 2-Ethylhexyl acrylate Ionization Acrylate Hexane Glycidyl methacrylate Butyl acrylate Methyl methacrylate Mass spectrometry Solvent Selected ion monitoring
Content Type	Text
Resource Type	Article
Subject	Analytical Chemistry Engineering Chemical Engineering

Sl.	Authority	Responsibilities	Communication Details
1	Ministry of Education (GoI), Department of Higher Education	Sanctioning Authority	https://www.education.gov.in/ict-initiatives
2	Indian Institute of Technology Kharagpur	Host Institute of the Project: The host institute of the project is responsible for providing infrastructure support and hosting the project	https://www.iitkgp.ac.in
3	National Digital Library of India Office, Indian Institute of Technology Kharagpur	The administrative and infrastructural headquarters of the project	Dr. B. Sutradhar bsutra@ndl.gov.in
4	Project PI / Joint PI	Principal Investigator and Joint Principal Investigators of the project	Dr. B. Sutradhar bsutra@ndl.gov.in Prof. Saswat Chakrabarti will be added soon
5	Website/Portal (Helpdesk)	Queries regarding NDLI and its services	support@ndl.gov.in
6	Contents and Copyright Issues	Queries related to content curation and copyright issues	content@ndl.gov.in
7	National Digital Library of India Club (NDLI Club)	Queries related to NDLI Club formation, support, user awareness program, seminar/symposium, collaboration, social media, promotion, and outreach	clubsupport@ndl.gov.in
8	Digital Preservation Centre (DPC)	Assistance with digitizing and archiving copyright-free printed books	dpc@ndl.gov.in
9	IDR Setup or Support	Queries related to establishment and support of Institutional Digital Repository (IDR) and IDR workshops	idr@ndl.gov.in

Scientific Opinion on the safety evaluation of the substance, (methyl methacrylate, butyl acrylate, styrene, glycidyl methacrylate) copolymer, CAS No. 37953-21-2, for use in food contact materials

Simultaneous determination of eight vitamin E isomers and α-tocopherol acetate in functional foods and nutritional supplements by gas chromatography – mass spectrometry

Simultaneous determination of 74 pesticide residues in Panax notoginseng by QuEChERS coupled with gas chromatography tandem mass spectrometry

Simultaneous Determination of Pyrethroid Insecticides in Foods of Animal Origins Using the Modified QuEChERS Method and Gas Chromatography-Mass Spectrometry.

Emulsion Copolymerization of Butyl Acrylate and Glycidyl Methacrylate: Determination of Monomer Reactivity Ratios (2010)

Emulsion Copolymerization of Butyl Acrylate and Glycidyl Methacrylate: Determination of Monomer Reactivity Ratios

International Journal of Mass Spectrometry 238 (2004) 279–286 Sequence dependent conformations of glycidyl methacrylate/butyl methacrylate copolymers in the gas phase (2003)

Simultaneous determination of cyanide and thiocyanate in plasma by chemical ionization gas chromatography mass-spectrometry (CI-GC-MS)

Determination of Selected Priority Pesticides in High Water Fruits and Vegetables by Modified QuEChERS and GC-ECD with GC-MS/MS Confirmation

Simultaneous determination of seven acrylates in food contact paper products by GC/MS and modified QuEChERS

Similar Documents

Scientific Opinion on the safety evaluation of the substance, (methyl methacrylate, butyl acrylate, styrene, glycidyl methacrylate) copolymer, CAS No. 37953-21-2, for use in food contact materials

Simultaneous determination of eight vitamin E isomers and α-tocopherol acetate in functional foods and nutritional supplements by gas chromatography – mass spectrometry

Simultaneous determination of 74 pesticide residues in Panax notoginseng by QuEChERS coupled with gas chromatography tandem mass spectrometry

Simultaneous Determination of Pyrethroid Insecticides in Foods of Animal Origins Using the Modified QuEChERS Method and Gas Chromatography-Mass Spectrometry.

Emulsion Copolymerization of Butyl Acrylate and Glycidyl Methacrylate: Determination of Monomer Reactivity Ratios (2010)

Emulsion Copolymerization of Butyl Acrylate and Glycidyl Methacrylate: Determination of Monomer Reactivity Ratios

International Journal of Mass Spectrometry 238 (2004) 279–286 Sequence dependent conformations of glycidyl methacrylate/butyl methacrylate copolymers in the gas phase (2003)

Simultaneous determination of cyanide and thiocyanate in plasma by chemical ionization gas chromatography mass-spectrometry (CI-GC-MS)

Determination of Selected Priority Pesticides in High Water Fruits and Vegetables by Modified QuEChERS and GC-ECD with GC-MS/MS Confirmation

Simultaneous determination of seven acrylates in food contact paper products by GC/MS and modified QuEChERS