NDLI: RRLC-MS/MS method for the quantitation of atractyloside in Fructus Xanthii (<i>Xanthium sibiricum</i>)

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RRLC-MS/MS method for the quantitation of atractyloside in Fructus Xanthii (Xanthium sibiricum)

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RRLC-MS/MS method for the quantitation of atractyloside in Fructus Xanthii (Xanthium sibiricum)

Content Provider	Royal Society of Chemistry (RSC)
Author	Feng, Yi Chen, Lulu Zeng, Xing Xie, Peishan Yang, Liu Xu, Shunjun
Copyright Year	2013
Abstract	Fructus Xanthii (Xanthium sibiricum) is used as a traditional Chinese medicine (TCM) but contains the toxin atractyloside. Historically the bur's spines are thought to be a reservoir of the toxins and removal of these spines theoretically reduced toxicity. However, this has not been proven and, furthermore, the Chinese Pharmacopoeia does not provide a quantitative method to evaluate the potential toxicity of this herb. Thus, the objective of this study was to provide a quantitative method using hydrophilic interaction liquid chromatography-tandem mass spectrometry to determine atractyloside content and concentration of Fructus Xanthii (Xanthium sibiricum) for the first time. Additionally, this method was validated and applied to evaluate the distribution and concentration of the atractyloside of this TCM in different plant parts including the spines, shell, seed-coat and seed kernel. The results of this analytical methodology applied to 27 samples of Fructus Xanthii (Xanthium sibiricum) demonstrated that this process improved sensitivity and accuracy and reduced the time commitment to evaluate this herb and others which potentially contain atractyloside. Furthermore, this study demonstrated that atractyloside is mainly stored in the seed kernel and not the spines as the historical thought.
Starting Page	2093
Ending Page	2097
Page Count	5
File Format	HTM / HTML PDF
ISSN	17599660
Volume Number	5
Issue Number	8
Journal	Analytical Methods
DOI	10.1039/c3ay26610a
Language	English
Publisher	Royal Society of Chemistry
Access Restriction	Open
Subject Keyword	Dahae Xanthium William Herbert (botanist) Seed Traditional Chinese medicine Fructus Xanthii Hydrophile Atractyloside Mass spectrometry Petroleum reservoir TCM
Content Type	Text
Resource Type	Article
Subject	Analytical Chemistry Engineering Chemical Engineering

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RRLC-MS/MS method for the quantitation of atractyloside in Fructus Xanthii (Xanthium sibiricum)