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Ethyl 2-(3-Methyl-5-oxo-4,5-dihydro-3H-benzo[e][1,4]diazepin-2-ylamino)benzoate
| Content Provider | MDPI |
|---|---|
| Author | Al-Said, Naim H. Al-Sghair, Ayat M. |
| Copyright Year | 2013 |
| Description | A simple route for synthesis of ethyl 2-(3-methyl-5-oxo-4,5-dihydro-3H-benzo[e][1,4]diazepin-2-ylamino)benzoate is developed. The present work involves condensation of 2-(2-nitrobenzamido)propanoic acid with ethyl anthranillate followed by the $H_{2}$/Pd/C reduction to give the amino ester which upon heating in DMF in the presence of $FeCl_{3}$ affords the title compound. The structure of the title compound was established on the basis of$ ^{1}$H-NMR,$ ^{13}$C-NMR and mass spectral data. |
| Starting Page | M811 |
| e-ISSN | 14228599 |
| DOI | 10.3390/m811 |
| Journal | Molbank |
| Issue Number | 4 |
| Volume Number | 2013 |
| Language | English |
| Publisher | MDPI |
| Publisher Date | 2013-12-12 |
| Access Restriction | Open |
| Subject Keyword | Molbank Organic Chemistry Benzo[e][1 4]diazepine Ferric Chloride Cyclization |
| Content Type | Text |
| Resource Type | Article |
