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Optimisation of AgNP Synthesis in the Production and Modification of Antibacterial Cellulose Fibres
| Content Provider | MDPI |
|---|---|
| Author | Smiechowicz, Emilia Niekraszewicz, Barbara Kulpinski, Piotr |
| Copyright Year | 2021 |
| Description | The main aim of the presented research is to determine the optimal conditions for the production of silver nanoparticles (AgNPs) in N-methylmorpholine-N-oxide (NMMO), which will potentially allow to obtain small nanoparticles with uniform diameter distribution. In this paper, NMMO is used in the fibre production process, both as a direct cellulose solvent and as an Ag+ reducing system. From an industrial point of view, this method is very promising because it allows to reduce the amount of used chemicals. The UV/Vis, DLS and TEM analysis proved that the synthesis temperature and time could play a key role in nanoparticle growth control in NMMO. It was found that the optimal conditions for AgNPs synthesis are 100 °C and 0.33 h. The estimations of the antibacterial activity of the fibres were completed. The applied AgNPs synthesis conditions allow to obtain antibacterial fibres with a wide range of applications, mainly in medicine. |
| Starting Page | 4126 |
| e-ISSN | 19961944 |
| DOI | 10.3390/ma14154126 |
| Journal | Materials |
| Issue Number | 15 |
| Volume Number | 14 |
| Language | English |
| Publisher | MDPI |
| Publisher Date | 2021-07-24 |
| Access Restriction | Open |
| Subject Keyword | Materials Nanocomposite Fibres Lyocell Antibacterial Cellulose Fibres Silver Nanoparticles N-methylmorpholine-n-oxide (nmmo) |
| Content Type | Text |
| Resource Type | Article |