NDLI: Synthesis of Cellulose-2,3-bis(3,5-dimethylphenylcarbamate) in an Ionic Liquid and Its Chiral Separation Efficiency as Stationary Phase

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Synthesis of Cellulose-2,3-bis(3,5-dimethylphenylcarbamate) in an Ionic Liquid and Its Chiral Separation Efficiency as Stationary Phase

Content Provider	MDPI
Author	Liu, Runqiang Zhang, Yijun Bai, Lianyang Huang, Mingxian Chen, Jun Zhang, Yuping
Abstract	A chiral selector of cellulose-2,3-bis(3,5-dimethylphenylcarbamate) (CBDMPC) was synthesized by reacting 3,5-dimethylphenyl isocyanate with microcrystalline cellulose dissolved in an ionic liquid of 1-allyl-3-methyl-imidazolium chloride (AMIMCl). The obtained chiral selector was effectively characterized by infrared spectroscopy, elemental analysis and 1H NMR. The selector was reacted with 3-aminopropylsilanized silica gel and the CBDMPC bonded chiral stationary phase (CSP) was obtained. Chromatographic evaluation of the prepared CSPs was conducted by high performance liquid chromatographic (HPLC) and baseline separation of three typical fungicides including hexaconazole, metalaxyl and myclobutanil was achieved using n-hexane/isopropanol as the mobile phase with a flow rate 1.0 mL/min. Experimental results also showed that AMIMCl could be recycled easily and reused in the preparation of CSPs as an effective reaction media.
File Size	427008
Ending Page	6168
Page Count	8
Starting Page	6161
File Format	PDF
e-ISSN	14220067
DOI	10.3390/ijms15046161
Journal	International Journal of Molecular Sciences
Issue Number	4
Volume Number	15
Language	English
Publisher Date	2014-04-11
Access Restriction	Open
Subject Keyword	1-allyl-3-methyl-imidazolium chloride synthesis Cellulose-2,3-bis(3,5-dimethylphenylcarbamate) high performance liquid chromatography chiral stationary phase enantioseparation
Content Type	Text
Resource Type	Article

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