NDLI: Effect of Annealing Temperature on the Optical Spectra of CdS Thin Films Deposited at Low Solution Concentrations by Chemical Bath Deposition (CBD) Technique

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Effect of Annealing Temperature on the Optical Spectra of CdS Thin Films Deposited at Low Solution Concentrations by Chemical Bath Deposition (CBD) Technique

Content Provider	MDPI
Author	Rizwan, Zahid Zakaria, Azmi Ghazali, Mohd Sabri Mohd Jafari, Atefeh Din, Fasih Ud Zamiri, Reza
Abstract	Two different concentrations of CdCl2 and (NH2)2CS were used to prepare CdS thin films, to be deposited on glass substrate by chemical bath deposition (CBD) technique. CdCl2 (0.000312 M and 0.000625 M) was employed as a source of Cd2+ while (NH2)2CS (0.00125 M and 0.000625 M) for S2− at a constant bath temperature of 70 °C. Adhesion of the deposited films was found to be very good for all the solution concentrations of both reagents. The films were air-annealed at a temperature between 200 °C to 360 °C for one hour. The minimum thickness was observed to be 33.6 nm for film annealed at 320 °C. XRD analyses reveal that the films were cubic along with peaks of hexagonal phase for all film samples. The crystallite size of the films decreased from 41.4 nm to 7.4 nm with the increase of annealing temperature for the CdCl2 (0.000312 M). Optical energy band gap (Eg), Urbach energy (Eu) and absorption coefficient (α) have been calculated from the transmission spectral data. These parameters have been discussed as a function of annealing temperature and solution concentration. The best transmission (about 97%) was obtained for the air-annealed films at higher temperature at CdCl2 (0.000312 M).
File Size	698368
Ending Page	1305
Page Count	13
Starting Page	1293
File Format	PDF
e-ISSN	14220067
DOI	10.3390/ijms12021293
Journal	International Journal of Molecular Sciences
Issue Number	2
Volume Number	12
Language	English
Publisher Date	2011-02-22
Access Restriction	Open
Subject Keyword	chemical bath deposition cadmium sulphide window layer air-annealing
Content Type	Text
Resource Type	Article

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