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Zn-nicotinate Complex - A Precursor For ZnO Nanoparticles
| Content Provider | Indian Institute of Science (IISc) |
|---|---|
| Author | Siddiqui, Kafeel Ahmad Mehrotra, Gopal K. |
| Copyright Year | 2013 |
| Abstract | A zinc-nicotinate complex has been prepared by direct reaction of zinc acetate and nicotinic acid in the presence of template tetramethylethylenediamine and is characterized by elemental analysis, FTIR, and TGA DTA. The Zn complex was a precursor for the synthesis of ZnO nanoparticles. A correlation of the thermal and spectral properties of the precursor complex with its structure has been discussed. Thermolysis under air was studied by thermogravimetry, and the resulting ZnO product was characterized by XRD and TEM, showing compact particles with a diameter of about 1750nm. |
| File Format | |
| Journal | PeerReviewed |
| Language | English |
| Publisher | Taylor and Francis Ltd |
| Publisher Date | 2013-05-01 |
| Access Restriction | Authorized |
| Subject Keyword | Solid State & Structural Chemistry Unit |
| Content Type | Text |
| Resource Type | Article |