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| Content Provider | IET Digital Library |
|---|---|
| Author | Wu, Xiang feng Zhang, Jie Zhuang, Ya fang Fu, Shi da Yu, Xiao ying |
| Abstract | Graphene oxide was prepared by a modified Hummers method in a Teflon-lined autoclave and then reduced by two different approaches. Alkaline reduction by sodium hydroxide as the control and synergetic reduction which combined sodium hydroxide and microwave irritation were conducted. The products were characterised by transmission electron microscopy, X-ray diffraction, thermo-gravimetric analysis, Fourier transform infrared spectroscopy and by atomic force microscopy. Results showed that the synergetic method possessed higher efficiency. Moreover, the as-prepared samples were monolayers (about 0.8 nm) and could decrease the solubility of ethyl cellulose in ethanol. |
| Starting Page | 804 |
| Ending Page | 806 |
| Page Count | 3 |
| Volume Number | 9 |
| e-ISSN | 17500443 |
| Issue Number | Issue 11, Nov (2014) |
| Alternate Webpage(s) | https://digital-library.theiet.org/content/journals/mnl/9/11 |
| Alternate Webpage(s) | https://digital-library.theiet.org/content/journals/10.1049/mnl.2014.0464 |
| Journal | Micro & Nano Letters |
| Publisher Date | 2014-11-06 |
| Access Restriction | Open |
| Rights Holder | © The Institution of Engineering and Technology |
| Subject Keyword | Alkaline Reduction Atomic Force Microscopy CO-NaOH Ethanol Ethyl Cellulose Fourier Transform Infrared Spectroscopy Fourier Transform Spectra Graphene Graphene Oxide Infrared And Raman Spectra in Inorganic Crystal Infrared Spectra Method of Nanofabrication And Processing Microwave Irritation Microwave Material Processing Mixing Modihed Hummers Method MonoLayer Nanocomposite Nanofabrication NanoParticle Nanosized Composite Material Nanotube And Nanostructured Material Reaction Mechanisms Reduction (Chemical) Segregation Sodium Compound Sodium Hydroxide Solid Surface Structure Solubility Specific Chemical Reactions Structure of Solid Clusters Synergetic Reduction Teflon-lined Autoclave Thermal Analysis Thermogravimetric Analysis Transmission Electron Microscopy X-Ray Diffraction |
| Content Type | Text |
| Resource Type | Article |
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