NDLI: Simultaneous Analysis of Multiple Classes of Antibiotics in Water and Soil Samples via Solid Phase Extraction and Liquid Chromatography-Tandem Mass Spectrometry

Content Provider	IEEE Xplore Digital Library
Author	Wei Hu Changsheng Guo Lili Ma Yuqiu Wang
Copyright Year	2010
Abstract	The analytical protocols were developed and tested for simultaneous determining three groups of antibiotics including four fluoroquinolones (FQs), three tetracyclines (TCs) and eleven sulfonamides (SAs), in water and soil samples. Solid phase extraction (SPE) was used to enrich and to clean up the aqueous samples. The potassium phosphate buffer and acetonitrile mixture solutions were used to extract the compounds from the soil samples. The target compounds were determined by liquid chromatography with tandem mass spectrometry (LC-MS/MS). The recoveries for the investigated antibiotics in water samples ranged from 60% to 105% with 2-14% of relative standard deviation (RSD). In soil samples, the recoveries were between 56% and 97% with 1-20% of RSD. The limits of quantification (LOQs) in water and soil samples were in the range of 1.2-10.6 ng/L and 0.2-29.6 µg/kg, respectively. Finally, the protocols were applied to environmental samples colleted from the Yuqiao Reservoir region. The FQs and SAs were detected in the water samples but none of target compounds were found in soil samples.
Starting Page	1
Ending Page	4
File Size	236151
Page Count	4
File Format	PDF
ISBN	9781424447121
ISSN	21517622
DOI	10.1109/ICBBE.2010.5518224
Language	English
Publisher	Institute of Electrical and Electronics Engineers, Inc. (IEEE)
Publisher Date	2010-06-18
Publisher Place	China
Access Restriction	Subscribed
Rights Holder	Institute of Electrical and Electronics Engineers, Inc. (IEEE)
Subject Keyword	Protocols Antibiotics USA Councils Humans Soil Solids Mass spectroscopy Reservoirs Water pollution Methanol
Content Type	Text
Resource Type	Article

Sl.	Authority	Responsibilities	Communication Details
1	Ministry of Education (GoI), Department of Higher Education	Sanctioning Authority	https://www.education.gov.in/ict-initiatives
2	Indian Institute of Technology Kharagpur	Host Institute of the Project: The host institute of the project is responsible for providing infrastructure support and hosting the project	https://www.iitkgp.ac.in
3	National Digital Library of India Office, Indian Institute of Technology Kharagpur	The administrative and infrastructural headquarters of the project	Dr. B. Sutradhar bsutra@ndl.gov.in
4	Project PI / Joint PI	Principal Investigator and Joint Principal Investigators of the project	Dr. B. Sutradhar bsutra@ndl.gov.in Prof. Saswat Chakrabarti will be added soon
5	Website/Portal (Helpdesk)	Queries regarding NDLI and its services	support@ndl.gov.in
6	Contents and Copyright Issues	Queries related to content curation and copyright issues	content@ndl.gov.in
7	National Digital Library of India Club (NDLI Club)	Queries related to NDLI Club formation, support, user awareness program, seminar/symposium, collaboration, social media, promotion, and outreach	clubsupport@ndl.gov.in
8	Digital Preservation Centre (DPC)	Assistance with digitizing and archiving copyright-free printed books	dpc@ndl.gov.in
9	IDR Setup or Support	Queries related to establishment and support of Institutional Digital Repository (IDR) and IDR workshops	idr@ndl.gov.in

Simultaneous determination of fluoroquinolone, sulfonamide, and trimethoprim antibiotics in wastewater using tandem solid phase extraction and liquid chromatography-electrospray mass spectrometry” in

Simultaneous determination of three classes of antibiotics in the suspended solids of swine wastewater by ultrasonic extraction, solid-phase extraction and liquid chromatography-mass spectrometry.

[Simultaneous determination of 23-antibiotics in mariculture water using solid-phase extraction and high performance liquid chromatography-tandem mass spectrometry].

[Simultaneous determination of 22 antibiotics in environmental water samples by solid phase extraction-high performance liquid chromatography-tandem mass spectrometry].

Simultaneous analysis of different classes of phytohormones in coconut (Cocos nucifera L.) water using high-performance liquid chromatography and liquid chromatography-tandem mass spectrometry after solid-phase extraction.

Preconcentration and Determination of Perfluoroalkyl Substances (PFASs) in Water Samples by Bamboo Charcoal-Based Solid-Phase Extraction Prior to Liquid Chromatography–Tandem Mass Spectrometry

Detection of 36 antibiotics in coastal waters using high performance liquid chromatography-tandem mass spectrometry

Determination of 4-Hexylresorcinol in Shrimp Samples by Solid Phase Extraction Ultra Performance Liquid Chromatography-Tandem Mass Spectrometry

Simultaneous quantification of several classes of antibiotics in water, sediments, and fish muscles by liquid chromatography-tandem mass spectrometry

Simultaneous Analysis of Multiple Classes of Antibiotics in Water and Soil Samples via Solid Phase Extraction and Liquid Chromatography-Tandem Mass Spectrometry

Similar Documents

Simultaneous determination of fluoroquinolone, sulfonamide, and trimethoprim antibiotics in wastewater using tandem solid phase extraction and liquid chromatography-electrospray mass spectrometry” in

Simultaneous determination of three classes of antibiotics in the suspended solids of swine wastewater by ultrasonic extraction, solid-phase extraction and liquid chromatography-mass spectrometry.

[Simultaneous determination of 23-antibiotics in mariculture water using solid-phase extraction and high performance liquid chromatography-tandem mass spectrometry].

[Simultaneous determination of 22 antibiotics in environmental water samples by solid phase extraction-high performance liquid chromatography-tandem mass spectrometry].

Simultaneous analysis of different classes of phytohormones in coconut (Cocos nucifera L.) water using high-performance liquid chromatography and liquid chromatography-tandem mass spectrometry after solid-phase extraction.

Preconcentration and Determination of Perfluoroalkyl Substances (PFASs) in Water Samples by Bamboo Charcoal-Based Solid-Phase Extraction Prior to Liquid Chromatography–Tandem Mass Spectrometry

Detection of 36 antibiotics in coastal waters using high performance liquid chromatography-tandem mass spectrometry

Determination of 4-Hexylresorcinol in Shrimp Samples by Solid Phase Extraction Ultra Performance Liquid Chromatography-Tandem Mass Spectrometry

Simultaneous quantification of several classes of antibiotics in water, sediments, and fish muscles by liquid chromatography-tandem mass spectrometry

Simultaneous Analysis of Multiple Classes of Antibiotics in Water and Soil Samples via Solid Phase Extraction and Liquid Chromatography-Tandem Mass Spectrometry