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| Content Provider | IEEE Xplore Digital Library |
|---|---|
| Author | Palizdar, M. Comyn, T.P. Ward, M.B. Brown, A.P. Harington, J. Kulkarni, S. Keeney, L. Roy, S. Pemble, M. Whatmore, R. Quinne, C. Kilcoyne, S.H. Bell, A.J. |
| Copyright Year | 2011 |
| Description | Author affiliation: Tyndall National Institute, University College Cork, Ireland (Kulkarni, S.; Keeney, L.; Roy, S.; Pemble, M.; Whatmore, R.) || Institute for Materials Research, University of Salford, UK (Quinne, C.; Kilcoyne, S.H.) || Institute for Materials Research, SPEME, University of Leeds LS2 9JT, UK (Palizdar, M.; Comyn, T.P.; Ward, M.B.; Brown, A.P.; Harington, J.; Bell, A.J.) |
| Abstract | Oxide materials which exhibit both ferroelectricity and ferromagnetism are of great interest for sensors and memory applications. Layered bismuth titanates with an Aurivillius structure, (BiFeO3)nBi4Ti3O12, can possess ferroelectric and ferromagnetic order parameters simultaneously. It has recently been demonstrated that one such example, Bi5Fe0.5Co0.5Ti3O15, where n = 1 with half the $Fe^{3+}$ sites substituted by $Co^{3+}$ ions, exhibits both ferroelectric and ferromagnetic properties at room temperature. Here we report the fabrication of highly-oriented polycrystalline ceramics of this material, prepared via molten salt synthesis and uniaxial pressing of high aspect ratio platelets. Electron backscatter images showed that there is a secondary phase within the ceramic matrix which is rich in cobalt and iron, hence this secondary phase could contribute in the main phase ferromagnetic property. The concentration of the secondary phase obtained from secondary electron microscopy is estimated at less than 2.5 %, below the detection limit of XRD. TEM was used to identify the crystallographic structure of the secondary phase, which was shown to be cobalt ferrite, CoFe2O4. It is inferred from the data that the resultant ferromagnetic response identified using VSM measurements was due to the presence of the minor secondary phase. The Remanent magnetization at room temperature was Mr ≈ 76 memu/g which dropped down to almost zero (Mr ≈ 0.8 memu/g) at 460 °C, far lower than the anticipated for CoFe2O4. |
| Starting Page | 1 |
| Ending Page | 4 |
| File Size | 860729 |
| Page Count | 4 |
| File Format | |
| ISBN | 9781457711626 |
| e-ISBN | 9781457711633 |
| e-ISBN | 9781457711619 |
| DOI | 10.1109/ISAF.2011.6013995 |
| Language | English |
| Publisher | Institute of Electrical and Electronics Engineers, Inc. (IEEE) |
| Publisher Date | 2011-07-24 |
| Publisher Place | Canada |
| Access Restriction | Subscribed |
| Rights Holder | Institute of Electrical and Electronics Engineers, Inc. (IEEE) |
| Subject Keyword | Temperature X-ray diffraction Powders Temperature measurement Cobalt Ceramics Ferrites microstructure multiferroic texture |
| Content Type | Text |
| Resource Type | Article |
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