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Direct Synthesis of (K0.5Na0.5)NbO3 Powders by Mechanochemical Method
| Content Provider | Hindawi |
|---|---|
| Author | Duc Van, Nguyen |
| Editor | Sun, Wen-Hua |
| Copyright Year | 2013 |
| Abstract | The synthesis and structural properties of lead-free piezoelectric (K0.5Na0.5)NbO3 powders prepared by mechanochemical method using Nb2O5, K2CO3, and Na2CO3 as starting materials were reported. X-ray diffraction, infrared spectroscopy, Raman spectroscopy, and scanning electron microscopy were used to characterize the prepared samples. Results showed that, for the first time, by selecting the milling speed of 600 rpm and the ball-to-powder weight ratio of 35 : 1 as milling parameters, pure (K0.5Na0.5)NbO3 crystalline phase was obtained directly in the as-milled samples after 5 h of milling time. The existence of a carbonato complex between CO32− and Nb5+ ions as an intermediate species of the formation of (K0.5Na0.5)NbO3 was also found. |
| Page Count | 4 |
| File Format | |
| ISSN | 16878434 |
| DOI | 10.1155/2013/230216 |
| Journal | Advances in Materials Science and Engineering |
| Volume Number | 2013 |
| e-ISSN | 16878442 |
| Language | English |
| Publisher | Hindawi Publishing Corporation |
| Publisher Date | 2013-08-06 |
| Access Restriction | Open |
| Rights License | This is an open access article distributed under the Creative Commons Attribution License, which permits unrestricted use, distribution, and reproduction in any medium, provided the original work is properly cited. |
| Content Type | Text |
| Resource Type | Article |
| Subject | Engineering Materials Science |