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| Content Provider | CSIR - National Institute of Science Communication and Policy Research (NISCPR) |
|---|---|
| Author | Vaidya, Rajiv Patel, Kaushik Patel, S. G. |
| Abstract | The zirconium triselenide (ZrSe₃) single crystal has been grown by chemical vapour transport technique using iodine as a transporting agent. The optimum condition for the growth of this crystal is given. The stoichiometry of the grown crystals was confirmed on the basis of energy disperse analysis by X-ray (EDAX) and remaining structural characterization was accomplished by X- ray diffraction (XRD) studies. The lattice parameters obtained from the XRD analysis were a= 5.45 Å, b=3.74 Å and c=9.44 Å. This crystal is found to possess monoclinic, layered structure. The X-ray density was found to be 5.63 g/cc and volume was calculated about 193.50 ų. The optical band gap of the as-grown crystal has been carried out with the help of optical absorption spectra in the range 700 - 1400 nm. |
| Ending Page | 516 |
| Starting Page | 514 |
| ISSN | 00195596 |
| e-ISSN | 09751041 |
| Journal | Indian Journal of Pure & Applied Physics (IJPAP) |
| Issue Number | 06 |
| Volume Number | 45 |
| Language | English |
| Publisher | Council of Scientific & Industrial Research (CSIR) |
| Publisher Date | 2007-06-01 |
| Access Restriction | Open |
| Subject Keyword | Optical Band Gap X-Ray Diffraction (XRD) EDAX Microstructural analysis ZrSe3 single crystal Optical absorption spectra Chemical vapour transport |
| Content Type | Text |
| Resource Type | Article |
| Subject | Physics and Astronomy |
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