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| Content Provider | The American Society of Mechanical Engineers (ASME) Digital Collection |
|---|---|
| Author | Kyle, M. Allen James, F. Klausner Eric, N. Coker Auyeung, Nick Mishra, Rishi |
| Copyright Year | 2013 |
| Abstract | This paper reports the synthesis, characterization and evaluation of different weight loadings of cobalt ferrite (CoFe2O4) in 8 mol% yttria-stabilized zirconia (8YSZ) via the co-precipitation method. Prepared powders were calcined at 1350 °C for 36 hours and 1450 °C for 4 hours in air. These powders were then formed into a porous structure using sacrificial pore formation via oxidation of co-mixed graphite powder. These formed structures obtained were then characterized using thermogravimetric analysis (TGA), X-ray diffraction (XRD), high temperature X-ray diffraction (HT-XRD), scanning electron microscopy (SEM) and energy-dispersive X-ray spectroscopy (EDS). Brunauer-Emmett-Teller (BET) surface area analysis was performed on the most promising of the structures before being subjected to 50 thermal reduction-CO2 oxidation (redox) cycles using TGA. Together, these results indicate that CoFe2O4-8YSZ can provide a lower reduction temperature, maintain syngas production performance from cycle to cycle, and enhance utilization of the reactive material within the inert support in comparison to iron oxide only structures. |
| Sponsorship | Advanced Energy Systems Division Solar Energy Division |
| File Format | |
| ISBN | 9780791855515 |
| DOI | 10.1115/ES2013-18254 |
| Volume Number | ASME 2013 7th International Conference on Energy Sustainability |
| Conference Proceedings | ASME 2013 7th International Conference on Energy Sustainability collocated with the ASME 2013 Heat Transfer Summer Conference and the ASME 2013 11th International Conference on Fuel Cell Science, Engineering and Technology |
| Language | English |
| Publisher Date | 2013-07-14 |
| Publisher Place | Minneapolis, Minnesota, USA |
| Access Restriction | Subscribed |
| Subject Keyword | Water Cycles Scanning electron microscopy Temperature Ferrites (magnetic materials) Carbon dioxide X-ray diffraction Iron High temperature X-ray spectroscopy Cobalt Syngas Weight (mass) Solar energy Graphite Oxidation Coprecipitation |
| Content Type | Text |
| Resource Type | Article |
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